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Cambridge IGCSE Chemistry · 0620

Chapter 4: Electrochemistry — Part 2

Topic 4.1b · Specific electrolysis reactions and electroplating

Electrolysis of Molten Compounds

In molten salts, a metal forms at the cathode and a non-metal forms at the anode.

  • Molten lead(II) bromide (PbBr2): Pb2+ ions are reduced to lead at the cathode, and Br- ions are oxidised to bromine at the anode.
  • Prediction: For any binary compound (containing only two elements) in a molten state, the positive ion forms the metal at the cathode, and the negative ion forms the non-metal at the anode.

Exam Traps

  • Do not apply aqueous rules to molten electrolytes — sodium metal forms from molten NaCl, not from brine.
  • Metal always at cathode, non-metal at anode for molten binary compounds — do not reverse the products.

Electrolysis of Aqueous Solutions

In aqueous solutions, water provides H+ and OH- ions which compete with the compound's ions at the electrodes.

  • At the Cathode: Hydrogen is produced if the metal is more reactive than hydrogen (e.g., sodium). The metal is produced only if it is less reactive than hydrogen (e.g., copper).
  • At the Anode: Oxygen and water are produced from OH- ions unless halide ions (Cl-, Br-, I-) are present, in which case the halogen is produced.
Electrolyte Product at Cathode Product at Anode Observations/Notes
Conc. Aqueous Sodium Chloride (Brine) Hydrogen gas (H2) Chlorine gas (Cl2) NaOH(aq) is left behind.
Dilute Sulfuric Acid Hydrogen gas (H2) Oxygen gas (O2) Requires inert electrodes.
Aq. Copper(II) Sulfate (Inert electrodes) Copper (brown deposit) Oxygen gas (bubbles) Blue colour of electrolyte fades as Cu2+ concentration decreases.
Aq. Copper(II) Sulfate (Copper electrodes) Copper (plating) Copper ions (Cu2+) Blue colour remains constant as the copper anode dissolves to replace ions.

Electroplating

Electroplating uses electrolysis to coat a thin layer of one metal onto another to improve appearance or resistance to corrosion.

  • Method: The cathode is the object to be plated; the anode is the plating metal; and the electrolyte contains ions of the plating metal.
  • Example: To plate steel with silver, use a silver anode and a silver nitrate electrolyte. Silver ions are reduced to silver atoms on the steel cathode.

Exam Traps

  • Do not place the object to be plated at the anode — metal ions are reduced (deposited) at the cathode.

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